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Institute for National Measurement Standards

Ionizing Radiation - Calibration Services

Ordering Calibrations Services

TheIonizing Radiation Standards Group develops and maintains Canada's primary measurement standards for ionizing radiation fields and provides calibrations based on these standards.

The Group works with standards and measurement techniques related to exposure and air-kerma in low-energy X-ray and 60Co beams, absorbed dose to water in 60Co beams and in electron and photon beams from linear accelerators, neutron fluence and dose equivalent, absorbed dose to tissue in a ß-ray field, and Fricke dosimetry. They also develop Monte Carlo techniques for the simulation of electron and photon transport in materials; and they participate in the development of dosimetry protocols for use in cancer radiotherapy clinics.

 Facilities
 Uncertainties
 Fees for Service

Contact:Dr. Carl Ross
Tel. (613) 993-2715

Facilities

The section is equipped with X-ray generators, two 60Co therapy units, radioactive sources, three - ray sources, an Elekta Precise clinical linear accelerator, and a 35 MeV electron linear accelerator.

The X-ray generators provide stable beams of X-rays at constant potentials from 10 kV to 300 kV. Exposure rates from 100 pA/kg to 60 µA/kg (about 1 mR/h to 15 R/min) can be selected, covering both protection and therapeutic levels. 60Co beams are standardized in terms of exposure, air-kerma, and absorbed dose. 60Co exposure rates between 400 nA/kg and 300 µA/kg (100 mR/min to 80 R/min) are available.

The electron linear accelerator is a 35 MeV high-current short-pulse machine. The accelerator can be run up to 50 MeV unloaded and can sustain an average current of 60 µA at 35 MeV.

A low energy "pretzel" magnet placed between sections makes available the full electron current at energies between 5 MeV and 12 MeV. At the end of the accelerator, a conventional 2-magnet steering system provides electron beams with well-known energies. A variety of targets, beam flatteners, collimator systems, scattering foil systems, beam current monitors, and beam steering systems allow a wide variety of clinical accelerator beams to be simulated. The accelerator can also be run with currents averaging less than a single electron per pulse. In addition to the provision of electron and photon beams for dosimetry, the electron linear accelerator is available to outside users.

The Elekta Precise Linac is a standard clinical radiotherapy machine with photon beams of 6, 10 and 25 MV and 5 electron beams with energies between 4 and 22 MeV. The linac delivers clinical dose rates of about 5 Gy/minute.

Uncertainties

The uncertainties quoted in the descriptions below are standard uncertainties, that is, they are at the one-standard-deviation level. They were obtained by assuming a normal distribution.

Fees for Service

Ordering Calibrations Services NEW procedures effective March 23, 2006.

A33-08-00-00
Custom Ionizing Radiation Standards Measurements or Services
Fee on request.
Contact Dr. Carl Ross for further information
A33-08-00-01
Handling Fee
$300
A charge is levied for any instrument or radioactive source that is found to be unsuitable for calibration. The fee covers inspection and return and is based on the work done prior to the discovery of the fault.

 Determination of Source Strengths
 Instrument Calibration
 Irradiations in Known Fields
 Use of NRC Irradiation Facilities
 Thermoluminescent Dosimetry (TLD)

Determination of Source Strengths (A33-08-01-01 to A33-08-01-04)
A33-08-01-01
60Co Therapy Source
$2750
The exposure or air-kerma rate from a 60Co therapy source at the client's location is measured by Council staff using an NRC calibrated cavity ion chamber.
A33-08-01-02
Additional 60Co Therapy Source
$365
Measurements of the exposure or air-kerma rate from additional sources will be made at a reduced rate per source when scheduled for testing at the same time and place as A33-08-01-01.
A33-08-01-03
Low-Activity 60Co Source
Fee on request
The exposure or air-kerma rate from low-activity 60Co sources is measured at NRC. This service is available by special arrangement only.
A33-08-01-04
Radioactive Neutron Source
$2055
This service measures the neutron flux from a radioactive neutron source. NRC no longer maintains a primary standard for neutron source strength. However, the Council does have several Am-Be neutron sources whose outputs and half-lives have been established. Using these sources and well characterized neutron long counters, the output from a client's neutron source can be established with a standard uncertainty of about 2% for sources with a spectrum similar to that of the Am-Be sources.



Instrument Calibration (A33-08-02-01 to A33-08-05-02)
A33-08-02-01
X-Rays
$1195
This service provides exposure and air-kerma calibration for one quality of radiation for one instrument and its probe using one instrument range.

The primary exposure and air-kerma standards at X-ray energies are two free-air chambers. The smaller of these covers X-rays produced by accelerating potentials up to 80 kV and the larger one covers X-rays up to 300 kV. This range of X-ray energies is produced by several special generators in which both the potential across the X-ray tube and the anode current are highly stabilized and accurately monitored. By varying the anode current and distance from the source, calibrations of instruments can be provided at exposure rates varying by six orders of magnitude, from therapy exposure rates (60µA/kg (15R/min)) to radiation protection rates (100 pA/kg (1 mRh)). A variety of beam filtrations is available and, after discussion with the client, NRC will match the client's end-use beam quality as accurately as possible during the calibrations.

The value of the exposure, or related air-kerma, typically has a standard uncertainty of 0.5% at the higher exposure rates, although the overall accuracy of the instrument's calibration factor also depends on the precision of the instrument being calibrated.

NRC exposure standards have been used in various international comparisons with other national standards laboratories. Agreement with the standards of NIST (National Institute of Standards and Technology) in the USA and the Bureau International des Poids et Mesures in France is within ±0.3% .
A33-08-02-02
Additional X-Rays
$250
Calibrations in additional beam qualities and/or instrument ranges will be performed at a reduced cost when scheduled at the same time as A33-08-02-01 and for the same instrument.
A33-08-03-01
60Co
$1195
Exposure and air-kerma calibrations, or absorbed dose to water calibrations, are carried out for one instrument and its probe using one instrument range. The primary exposure standard for gamma-radiation from 60Co is a carbon-walled cavity ion chamber. Extensive work has been done concerning the correction factors required for cavity chamber exposure standards, in particular the point of measurement correction factor and the wall attenuation and scatter correction factor.

The laboratory has two 60Co teletherapy heads with calibrated outputs. The older unit produces exposure rates at 1 m of about 20 µA/kg (5 R/min). In conjunction with a precision irradiation timer designed and built at NRC, this unit can deliver accurately-known exposures down to less than 25 µC/kg (100 mR). This unit is used primarily for the calibration of radiation protection instruments. The newer unit produces an exposure rate at 1 m of about 300 µA/kg (80 R/min), which is more typical of clinical units and is used primarily for the calibration of radiation therapy instruments.

For both units, the exposure rates are known with a standard uncertainty of 0.5% (one standard deviation) although the overall accuracy of a calibration factor also depends on the precision of the instrument.

The 60Co units at NRC are former therapy units and thus the spectrum from these units is similar to that used in therapy situations. Measurements and Monte Carlo simulations done at the Council indicate that over 25% of the photon fluence in the beams of these machines consists of scattered photons and these contribute about 15% of the exposure in the beam.

The 60Co air kerma standard at NRC has been compared to the standards in several other national standards laboratories, such as PTB (Physikalisch Technische Bundesanstalt) in Germany and the Bureau International des Poids et Mesures in France, and found to agree within 0.2%, although air kerma rates measured using NRC calibrations are 0.6% larger than those based on calibrations from NIST.

The standard for absorbed dose to water in a 60Co beam is a sealed water calorimeter. The instrument measures the radiation-induced temperature rise at a point in a water phantom.

The absorbed dose to water rate is known at 5 cm depth in a water phantom irradiated by a 10 x 10 cm2 beam, with the surface of the phantom at 1 m from the source. Based on this knowledge, waterproof ion chambers can be calibrated directly in terms of absorbed dose to water by being placed in the water phantom.

The dose rates at the point of calibration are about 8 cGy/min and 60 cGy/min on the two 60Co units discussed above. The standard uncertainty in the absorbed dose rate is 0.6%.
A33-08-03-02
Additional 60Co
$250
Calibrations on additional instrument ranges will be performed at a reduced cost when done at the same time as A33-08-03-01.
A33-08-04-01
Neutrons
$1485
A neutron survey meter is calibrated using an Am-Be source of known output. Using this source, and a knowledge of its spectrum (average energy 4.4 MeV), NRC can provide calibrations of neutron remmeters in a field of roughly
20 µSv /h  (2 mrem h-1).
A33-08-05-01
ß-Rays
Fee on request
Absorbed dose to tissue calibration of a direct reading ß dosimeter is performed in fields from 204Tl, 90Sr+90Y, and 147Pm ß sources at a variety of specified distances.

The primary standard for ß-ray absorbed dose is an extrapolation ion chamber built at NRC following a design developed by PTB in Germany. With this chamber, the absorbed dose to tissue at a variety of depths in a tissue equivalent phantom has been determined at a variety of distances from 204Tl, 90Sr+90Y, and 147Pm ß sources. At the calibration positions, the mean energies of these ß sources have been determined to be 300 keV, 670 keV, and 70 keV respectively. The dose rates span more than three orders of magnitude and have been determined with a standard uncertainty of 2%. The measurements agree well with independent calibrations carried out on the same set of sources by PTB.

These sources can be used to calibrate radiation protection instrumentation although great care must be taken in interpreting the results since calibration factors are very geometry dependent; that is, the calibration factor usually changes as a function of distance from the ß source because the ß spectrum changes due to slowing and scattering in the air.

This calibration service is available by special arrangement only. Only the 90Sr+90Y calibrations are routinely calibrated.
A33-08-05-02
Additional ß-Rays
Fee on request
Additional distance calibrations for the ß dosimeter used in A33-08-05-01 can be performed at the same time at a reduced rate per distance calibrated. This service is available by special arrangement only.

Irradiations in Known Fields (A33-08-07-01 to A33-08-07-02)
A33-08-07-02
Irradiation of Material in 60Co, beta, and X-Ray Fields
Fee on request
Material is irradiated to a known dose or exposure in 60Co and X-ray fields.

The Council's X-ray generators, 60Co teletherapy units, and sources used in the various standards are available for irradiation purposes. NRC also has a variety of other sources with varying strengths, for example, a 60Co Gamma-cell with a dose rate of 8 Gy/minute and a variety of calibrated weak 60Co and radium sources for calibrating radiation protection instrumentation.

This service is available by special arrangement only.

Use of NRC Irradiation Facilities (A33-08-08-01 & A33-08-10-01)
A33-08-08-01
35 MeV linear Accelerator
$(/hr) 500

The group has a 35 MeV linear accelerator which provides electron beams with energies between 5 MeV and 35 MeV with average beam currents up to 60 µA. This can be used to produce either electron or photon beams in a wide variety of configurations. The linear accelerator beam is available on an hourly basis. A minimum of four hours must be reserved.

A33-08-10-01
Use of 60Co or X-Ray Unitsr
$(/hr) 100

The 60Co and X-ray unit facilities at NRC are available on an hourly basis. A minimum of four hours must be reserved.



Thermoluminescent Dosimetry (TLD)

Quality Assurance Service (A33-08-11-01 to A33-08-11-04)

60Co Dosimetry

Facilities are available at NRC for quality assurance testing of personal dosimetry systems, most of which use TLD. The service provided by the Council involves irradiating a batch of up to 150 TLDs free in air in a 60Co beam to a known exposure or air-kerma of between 30 µC/kg (1mGy to air) and 30 mC/kg (1 Gy to air). The irradiated dosimeters are returned to the client dosimetry services which process them and report their results for the exposure or air-kerma to NRC. NRC compares the dosimetry service values to the Council's values and reports the results simultaneously to the Atomic Energy Board of Canada and to the dosimetry services.

A33-08-11-01
$9295
This service covers the first use of the Co facilities in a single calendar year.
A33-08-11-02
$447.50
Each subsequent use of the Co facilities in the same calendar year is charged at a reduced rate per usage.

X-Ray Dosimetry

Facilities are available for X-Ray dosimetry similar to the 60Co dosimetry service (A33-08-11-01 and A33-08-11-02) described above. The radiation procedure is consistent with the requirements outlined in Appendix H of the Independent Test Specifications for Dosimetry Services: X-radiation, in the Regulatory Standards S-106(e), Technical and Quality Assurance Standards for Dosimetry Services, published on March 20, 1998, by the Atomic Energy Control Board. The procedure is tailored to meet the client's requirements and the fees are set accordingly. NRC values and the client's measured values for exposure (air kerma) are sent to the Provincial Radiation Dosimetry Review Committee.

A33-08-11-03
$9295
This service covers the first use of the X-Ray facilities in a single calendar year.
A33-08-11-04
$447.50
Each subsequent use of the X-Ray facilities in the same calendar year is charged at a reduced rate per usage.

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