Chemistry, Generation and Treatment of Thiosalts
Orlando Dinardo
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CANMET Reports
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These reports have not undergone detailed a technical review by the Mines and Mineral Sciences Laboratories (MMSL). The content does not necessarily reflect the views and policies of Natural Resources Canada. Mention of trade names or commercial products does not constitute endorsement for use.
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1
Bartels, K.
Chemical Abstract Index compilation for thiosalts and related compounds.
Report MRP/MSL 77-214 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
2
Bartels, K.
Evaluation of the destruction of thiosalts by electro-oxidation.
Report MRP/MSL 79-126 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
3
Bartels, K. and Farrell, D.M.
Infrared spectra and molecular (ionic) structures of thiosalts and related compounds.
Report MRP/MSL 80-145 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
4
Dinardo, O.
Literature review of thiosalt oxidation by thiobacilli species.
Report MRP/MSL 78-197 (LS), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
5
Dutrizac, J.E.
Meeting with Noranda personnel concerning thiosalts and the Noranda contract on the evaluation of thiosalt treatment options.
Report MSL-INT 84-1, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1984.
6
Dutrizac, J.E.
Meeting with Professor G.E. Rempel, University of Waterloo, Waterloo Ontario, Sept. 20, 1983.
Internal report MSL-INT 83-30, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1983
7
Dutrizac, J.E.
Preliminary evaluation of reverse osmosis and electrodialysis for the treatment of thiosalt effluents.
Report MRP/MSL 78-216 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
8
Dutrizac, J.E.
Thiosalt seminar program, Pointe Claire, Quebec, May 11, 1981.
Report MSL-INT 81-21, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
9
Dutrizac, J.E., Francis, D.J., Rolia, E. and Steger, H.
Visit to Noranda Research Centre, Pointe Claire, Quebec.
Report MRP/MSL 76-128 (FT), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
10
Dutrizac, J.E. and O'Reilly, J.B.
Listing of documents produced as part of CANMET's thiosalt program.
Division report MRP/MSL 82-18 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1982.
11
Francis, D.J.
Disposal of thiosalt effluents from the Brunswick Mining and Smelting Corp. no. 12 mine: a preliminary assessment of a pipeline to the sea.
Division report MRP/MSL 77-126 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
12
Haque, K.E. and Dinardo, O.
Thiosalts removal from mine/mill effluent by halide mediated electro-oxidation.
Division report MMSL 96-039 (OP&J) Draft, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1996.
13
Hitchen, A.
Preparation of potassium tetrathionate and potassium trithionate for studies of the thiosalt problem in mining effluents.
Report MRP/MRL 76-279 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
14
Hitchen, A. and MacPherson, D.R.
Spectrophotometric determination of micro amounts of thiosulphate and tetrathionate by cyanolysis and solvent extraction.
Division report MSL/INT81-12 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
15
Hitchen, A. and Smith, C.W.
Review of analytical methods for the determination of polythionates, thiosulphate, sulphite and sulphide in mining effluents.
Division report MRP/MSL 76-208 (LS), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
16
Kelly, F.J.
Estimated capital and operating costs for an effluent pretreatment plant.
Report MSL/INT 78-79, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
17
Makhija R.
Determination of polythionates and thiosulphate in mining effluents and mill circuit samples.
Report MRP/MRL 76-361 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
18
Makhija R. and Hitchen, A.
Titrimetric determination of sulphate, thiosulphate and polythionates in mining effluents.
Report MRP/MRL 76- (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
19
McCready, R.G.L.
Metabolism of the thiobacilli.
Report MRP/MSL 78-57 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
20
Riveros, P., Wong, E.W., MacKinnon, D.J., Haque, K.E., Giziwicz, E.A. and Kondos, P.D.
Chloride mediated electro-oxidation of cyanide.
Report No. MSL-INT 95-049 (ITR), CANMET, Natural Resources Canada, Ottawa, ON, 1995.
21
Rolia, E.
Analyses for sulphate and individual thiosalts in tailing-pond water and in mill solutions from Brunswick Mining and Smelting, Bathurst, New Brunswick.
Division report MRP/MSL 77-46 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
22
Rolia, E.
Generation of thiosalts in the flotation mill at Brunswick Mining and Smelting Corporation Limited, Bathurst, New Brunswick.
Division report MRP/MSL 78-46 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
23
Rolia, E.
Interim report on the production of thiosalts during the grinding of a pyritic Zn-Pb-Cu sulphide ore from Brunswick no. 12 mine.
Division report MRP/MSL 77-142 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
24
Rolia, E.
Kinetics of decomposition of thiosalts by metallic iron.
Division report MRP/MSL 81-75 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
25
Rolia, E.
Methods of analyses for sulphate, for individual thiosalts, and for elemental sulphur produced during the oxidation of sulphide ores.
Division report MRP/MSL 77-21 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
26
Rolia, E.
Oxidation of thiosalts in strongly alkaline media.
Division report MRP/MSL 81-132 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
27
Rolia, E.
Oxidation of thiosalts with hydrogen peroxide.
Division report MRP/MSL 84-144 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1984.
28
Rolia, E.
Study of the comparative rates of thiosalt generation from cleaned sulphide mineral concentrates and BMS ore during agitation in a flotation cell.
Division report MRP/MSL 80-23 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1980.
29
Rolia, E.
Towards an environmental standard for thiosalt effluents.
Division report MRP/MSL 83-130 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1983.
30
Rolia, E.
Visit to Brunswick Mining and Smelting Corporation Limited, Bathurst, New Brunswick. June 22-24, 1977.
Report MRP/MSL 77-25 (FT), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
31
Rolia, E. and Barbeau, F.
Analytical procedure for individual thiosalts and for sulphate in flotation mill solutions.
Division report MRP/MSL 79-70 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
32
Rolia, E. and Barbeau, F.
Contribution of sulphur dioxide to thiosalt generation in the flotation mill of Brunswick Mining and Smelting Corporation Limited.
Report MRP/MSL 78-173 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
33
Rolia, E. and Barbeau, F.
Effect of pH and retention time on the degradation of thiosalts.
Division report MRP/MSL 79-8 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
34
Rolia, E. and Barbeau, F.
Oxidation of thiosalts by: SO2 plus air, charcoal plus air, and chlorine.
Division report MRP/MSL 79-85 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
35
Rolia, E. and Barbeau, F.
Thiosalt generation during the production of bulk concentrate from Brunswick Mining and Smelting Corporation ore.
Report MRP/MSL 79-74 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
36
Rolia, E. and Barbeau, F.
Thiosalt generation in Heath Steele Mines Limited concentrator: comparison of thiosalt generation and of effluent treatment at Brunswick Mining and Smelting Corporation Limited.
Division report MRP/MSL 78-159 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
37
Rolia, E. and Chakrabarti, C.L.
Kinetics of decomposition of tetrathionate and thiosulphate in alkaline media.
Division report MRP/MSL 81-33 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
38
Rolia, E. and Tan, K.G.
Generation of thiosalts in mills processing complex sulphide ores.
Division report MRP/MSL 78-159 (Draft), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1985
39
Rolia, E. and Tan, K.G.
Oxidation of thiosulphate by hydrogen peroxide in alkaline solutions.
Division report MRP/MSL 84-84 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1984.
40
Rolia, E. and Tan, K.G.
Thiosalt generation parameters in flotation mill solutions.
Division report MRP/MSL 85-32 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1985.
41
Sastri, V. S.
Reverse osmosis and its application in the treatment of mining waste effluents.
Division report MRP/MSL 79-49 (OP), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
42
Sastri, V.S.
Reverse osmosis treatment of thiosalt solutions.
Division report MRP/MSL 77-401 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1977.
43
Silver, M.
Factors affecting the oxidation of thiosalts by thiobacilli.
Division report MRP/MSL 80-160 (OP&J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1980.
44
Silver, M.
Parameters for the operation of bacterial thiosalt oxidation ponds.
Division report MRP/MSL 85-25 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1985
45
Silver, M. and Dinardo, O.
Factors affecting the oxidation of thiosalts by thiobacilli.
Division report MRP/MSL 80-160 (OP&J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1980.
46
Smith, C.W. and Hitchen, A.
Aqueous solution chemistry of polythionates and thiosulphate: a review of formation and degradation pathways.
Division report MRP/MSL 76-223 (LS), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
47
Steger, H.F.
Effect of temperature, pH, particle size and air flow on the formation of thiosalts in sulphide mineral suspension.
Division report MRP/MSL 78-213 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1978.
48
Steger, H.F. and Desjardins Leo E.
Oxidation of sulphide minerals. III. Determination of sulphate and thiosulphate in oxidised sulphide minerals.
Division report MRP/MSL 76-316 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1976.
49
Stewart, J.M. and Szymanski, J.T.
Crystal structure of potassium terathionate, K2 S4 O6.
Division report MRP/MSL 79-10 (J), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
50
Stewart, J.M. and Szymanski, J.T.
Redetermination of the crystal structure of potassium trithionate, K2 S3 O6.
MRP processing contribution 105, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1979.
51
Tan, K.G.
Chlorination of thiosalt-containing effluents.
Division report MRP/MSL 84-135 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1984.
52
Tan, K.G. and Rolia, E.
Chemical oxidation methods for the treatment of thiosalt-containing mill effluents.
Division report MRP/MSL 85-59 (J) Draft, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1985.
53
Tan, K.G. and Rolia, E.
Ozonation of thiosalt-containing effluents.
Division report MRP/MSL 84-152 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1984.
54
Wasserlauf, M. and Dutrizac, J.E.
Chemistry, generation and treatment of thiosalts in milling effluents - a non-critical summary of CANMET investigations 1976 - 1982.
CANMET Rep. 82-4E, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1982.
55
Wasserlauf, M. and Dutrizac, J.E.
Overview of CANMET's project on the chemistry, generation and treatment of thiosalts in milling effluents.
Division report MRP/MSL 83-2 (J) Draft, CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1983.
56
Wong, W.S.
Preliminary capital and operating cost estimates for the catalytic oxidation of thiosalts.
Division report MRP/MSL 81-112 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1981.
57
Wong, W.S.
Preliminary capital and operating cost estimates for the pressure oxidation and metallic iron reduction processes for thiosalt removal.
Division report MRP/MSL 82-26 (TR), CANMET, Energy, Mines and Resources Canada, Ottawa, ON, 1982.
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64
Belcher, R., Liao, Sarah Sau-Tung and Townsend, Alan
Titrimetric determination of thiocyanate and thiosulphate ions by oxidation with iodine in alkaline solution.
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65
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Chemical processes in abandoned sulphide tailings dumps and environmental implication for northeastern New Brunswick.
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Radiochemical method for determining cyanides in solution.
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Byerley, John J., Fouda, Safaa A. and Rempel, Garry L.
Kinetics and mechanism of the oxidation of thiosulphate ions by copper (II) ions in aqueous ammonia solution.
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70
Byerley, John J., Fouda, Safaa A. and Rempel, Garry L.
Oxidation of thiosulfate in aqueous ammonia by copper (II) oxygen complexes.
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Callaghan, Fergal
Living with leachate.
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73
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Catalyzed air oxidation for treatment of thiosalt effluents.
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74
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Effect of ligand ratio on the catalytic activity of poly(4-vinylpyridine)-copper (II) chelate in the oxidation of thiosalts by molecular oxygen.
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75
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Ion exchange sorption of thiosulfate and tetrathionate on protonated poly(4-vinyl pyridine).
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76
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Polymer supported metal complexes as catalysts for oxidation of thiosalts by molecular oxygen I:poly (4-vinyl pyridine) - Cu (II) complex.
Journal of Molecular Catalysis, vol. 12, no. 2, pp. 197-212, 1981.
77
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Polymer supported metal complexes as catalysts for oxidation of thiosalts by molecular oxygen II: copper (II) complex of polystyrene-bound 2,2'-bipyridine.
Journal of Molecular Catalysis, vol. 8, no. 4, pp. 339-351, 1980.
78
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Polymer supported metal complexes as catalysts for oxidation of thiosalts by molecular oxygen III: comparative kinetic studies with poly(4-vinyl pyridine)-Cu(II) complex.
Journal of Molecular Catalysis, vol. 11, pp. 9-21, 1981.
79
Chanda, M., O'Driscoll, K.F. and Rempel, G.L.
Polymer supported metal complexes as catalysts for oxidation of thiosalts by molecular oxygen IV: quarternised poly(4-vinyl pridine) complexes with Cu2+ as template.
Journal of Molecular Catalysis, vol. 12, pp. 197-211, 1981.
80
Chanda, M., Grinshpun, A., O'Driscoll, K.F. and Rempel, G.L.
Polymer supported metal complexes as catalysts for oxidation of thiosalts by molecular oxygen V: the polythiosemicarbazide - Cu(II) complex.
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81
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Catalysed air oxidation of thiosulfate and tetrathionate for pollution abatement.
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